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Reproducible scale-up of medicinal chemistry reactions

Case study on heating system used to scale up syntheses



Parallel evaporation of high boiling solvents

DrySyn Spiral Evaporator offers fast and effective parallel evaporation in tubes or vials without solvent bumping



High throughput chemistry in microwave vials

Enables clean, safe synthesis without the hazards or problems associated with silicon oil baths or heating mantles



Heating block for chemists

Converts any standard hotplate stirrer into a reaction block platform for a single flask from 500ml down to 5ml



Laboratory tools for sustainable synthetic organic chemistry

Asynt DrySyn heating block range provide a safer and cleaner way of heating reactions



Single experiment heating block

DrySyn UNO designed to enable chemists to perform heated and stirred experiments in single flasks and vials



Heating block starter kit

Asynt has introduced a new starter kit based upon its DrySyn Classic heating blocks



Air condenser demonstrates high operational safety

For synthetic experiments a reflux condenser is an essential tool for both research and teaching chemistry



Inert purge parallel synthesiser

Large surface area of these glass reaction tubes enables the DrySyn Octo to be used for air cooled gentle reflux reactions



Compact eight-position parallel synthesiser

The compact DrySyn Octo parallel synthesiser accommodates low cost consumable reaction tubes each with a working volume of 5-6ml



Non-ducted cabinet

Filtration and fume cabinets enable development of infectious disease diagnostics



High throughput chemistry in microwave vials

Enables clean, safe synthesis without the hazards or problems associated with silicon oil baths or heating mantles



Reliable control of exothermic reactions

The DrySyn SnowStorm ONE from Asynt is designed to provide reliable temperature control of exothermic reactions



Exhaust trap for lab vacuum pumps

Traps additional vapours escaping from rotary evaporators ensuring a greener and more 'worker safe' environment



Guide to safe use of laboratory heating blocks

Developed to enable laboratory personnel to more safely use heating block systems



High pressure parallel reactor

MultiCell reactor offers users the ability to undertake 10 x 30 ml reactions in parallel at pressures of up to 50 bar and temperatures up to 200°C



How choice of reactor vessel affects reaction performance

Data is presented for vacuum jacketed and non-vacuum jacketed reaction vessels connected to a Julabo Presto A30 temperature control system



Mesoscale segmented flow reactor

Liquid segmented mesoscale tubular reactor runs for 5 hours without fouling issues and with instant recovery of solids



Optimised condenser for small scale reactions

For small scale synthetic chemical reactions performed in 5, 10, and 25ml flasks



Scientific reports compare air and water condensers

Water-driven condensers can use a large amount of water which is wasteful/expensive



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